FOSSVolkswagen Next GenerationKjeltec 8400Automatic kieldahl apparatus
Product model:Kjeltec™ 8400
(021: 676221675)
Kjeltec 8400Innovation point:
1.Specialized computer software can be used for managementKjeltec 8400Fully automatic Kjeldahl nitrogen analyzer and sampler system, according toGLPThe requirement is to provide fast and reliable sample registration and traceability, including seamless connection with any manufacturer's scales, printers, and computers.
2.Currently, there are only nitrogen analyzers available in the marketFOSSThe nitrogen analyzer adoptsSAfE/DelayTwo distillation modes.SAfEThe mode (steam balance addition mode) isFOSSA unique patented technology. A brief overview of the two distillation modes is as follows:
The working steps of the delay mode are as follows: adding water, adding alkali, adding receiving liquid, and passing steam; This may cause water alkali acid stratification in the distillation tube before steam is passed. Once steam is introduced to provide heat, a violent reaction will occur, and in the case of stratification, it will cause the crystallization at the bottom of the distillation tube (due to the formation of saturated solution and crystallization during the cooling digestion process) to become insoluble. Crystalline particles may be pushed up by the pressure generated by violent reactions, blocking steam pipes and distillation pipelines. Simultaneously, intense reactions can cause strong acids and bases to impact the distillation head, increasing the degree of corrosion and shortening the lifespan of the distillation head.
The working steps of the steam balance addition mode are: adding water, passing steam, adding receiving liquid, and slowly adding alkali. Before adding the alkali reaction, steam was introduced to effectively mix the acid and water, reducing the concentration of the acid while dissolving the crystals at the bottom of the distillation tube. When adding alkali slowly, the reaction becomes calm. It will not cause significant boiling and effectively protects the distillation head. At the same time, the steam volume is large and the distillation efficiency is high.
3.Explanation on Condensation Temperature Monitoring
The ammonia produced during distillation needs to be effectively condensed before it can be converted into ammonia water and completely absorbed by boric acid. Poor condensation effect may lead to nitrogen loss.FOSSThe nitrogen analyzer has a distillation temperature sensor: it directly measures the temperature of the distillate. Once the temperature exceeds the limit, it will automatically alarm and accurately reflect whether ammonia has been lost.
4.Explanation on Automatic Sample Injector and Injection Method
8400The connected automatic sampler is20Bit Or60At most, other brands only have20Position, therefore from an efficiency perspective8400Can provide high analytical skills.
As for the injection method,8400The sampler uses mechanical injection, and after digestion, only the digestion tube holder needs to be directly placed into the sampler, and then the digestion tube is directly sent into it8400Distillation titration is carried out inside the main unit of the nitrogen analyzer. After titration, the mechanical device will remove the analyzed digestion tube and send it to the next digestion tube. Throughout the entire analysis process, there was no transfer of the digestive tract and sample, ensuring the accuracy of the analysis.
To meet the needs of different users, we can also provide8100、8200Kjeldahl nitrogen determination system.
Kjeltec 8400Technical parameters:
1.Measurement range:0.1-200mgnitrogen
2.Distillation time:3.5minute/Sample(30mgNitrogen)
3.Distillation capacity:~40ml/minute
4.Titration accuracy:2.4ul/pace
5.Reproducibility:RSD1%
6.rate of recovery:>99.5%(1-200mgNitrogen)
7.Data storage:40Batch (software can store without restrictions)
8.Test tube emptying:200mlexist10Complete within seconds
9.Reagent pump volume:0-150ml,10ml/level
10.Delay time:0-1800s
11.SAfE:0-15s
12.Injector capability:20position/60position
Kjeltec 8400Main features:
1.Officially approved color titration system(AOAC, EPA, DIN, ISO,GBWaiting for clear regulations)
2.Fully automatic distillation process: including sample dilution, addition of alkaline and absorbent solutions, distillation, titration, calculation, reporting, and emptying of digestion tubes
3.Patent balanced steam addition* (SAfE)Technology ensures acid in the digestive tract/Distillation safety during salt cake production
4. Temperature control during distillation process can ensure accurate results
5.A series of safety oriented sensors in the system:1Distillation tube in place2Safety gate3Front panel4Reagent level5Add liquid level and6Overpressure of steam generator ensures comprehensive user safety
6. optional20/60Sample injector for automatic operation without the need for human supervision.
7.The positive pressure titrant delivery system, self-cleaning titration cylinder and self correcting anti-aging colorimetric elements provide a titration system with unparalleled accuracy.
8.Optional data management softwareCompassFully computer-controlled sample registration and reporting can be achieved.
9.The intelligent cooling water control system automatically adjusts the flow rate of tap water to reduce costs.
The following are andKjeltec 8400Accessories and consumables for matching use, available for selection:
The following old item numbers(QQ181224356)
15270057 Copper catalyst,4.5g K2SO4and0.5g CuSO4·5H2O,1000a flat/box
15270018 Copper catalyst,3.5g K2SO4and0.4g CuSO4·5H2O,1000a flat/box
The following new item number (021: 676221675)
60046518 Copper catalyst,4.5g K2SO4and0.5g CuSO4·5H2O,1000a flat/box
60046515 Copper catalyst,3.5g K2SO4and0.4g CuSO4·5H2O,1000a flat/box
10014311 Straight digestive tract,100ml,8/wrap
10014312 Straight digestive tract,100ml,20/wrap
10000735 Straight digestive tract,100ml,40/wrap
100333/10014278Straight digestive tract,250ml,8/wrap
10000158 Straight digestive tract,250ml,20/wrap
60025134 Straight digestive tract,400ml,20/wrap
10000787 750mlDirect distillation tube,6/wrap
10014245 Digestive duct rack8position250ml
10014240 Digestive duct rack20position250ml
10000056 Digestive tube connector-250ml
10000897 Digestive tube clamp
60028296 Distillation head
60031626 alkali pump
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